2-(Ph₃P=NCH₂)(C₅H₄N)

Base Information

Chemical Name:2-(Ph₃P=NCH₂)(C₅H₄N)
CAS No.:609770-37-8
Molecular Formula:C₂₄H₂₁N₂P
Molecular Weight:368.418
Hs Code.:

2-(Ph<sub>3</sub>P=NCH<sub>2</sub>)(C<sub>5</sub>H<sub>4</sub>N)

Synonyms:2-(Ph₃P=NCH₂)(C₅H₄N)

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Chemical Property of 2-(Ph₃P=NCH₂)(C₅H₄N)

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Technology Process of 2-(Ph₃P=NCH₂)(C₅H₄N)

There total 1 articles about 2-(Ph₃P=NCH₂)(C₅H₄N) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 586-98-1
2-Hydroxymethylpyridine

: 609770-37-8
2-(Ph₃P=NCH₂)(C₅H₄N)

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / chloroform / 3 h / Cooling with ice

2: sodium azide; sodium iodide / acetonitrile / 24 h / Reflux

3: toluene / 8 h / Reflux

With thionyl chloride; sodium azide; sodium iodide; In chloroform; toluene; acetonitrile;
DOI:10.1039/c4ob01176g

Reference yield: 80.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 609770-37-8
2-(Ph₃P=NCH₂)(C₅H₄N)

: 609770-40-3
[(Ph₃PN-CH₂-2-NC₅H₄)PdCl₂]

Guidance literature:: In toluene; under N2; the ligand in toluene added to toluene suspn. of PdCl2(PhCN)2;soln. stirred overnight; solvent vol. reduced; Et2O added; ppt. filtered; solid washed with Et2O,dried in vacuo, and recrystd. by slow diffusion of satd. CH2Cl2 layer i nto hexane; elem. anal.;
DOI:10.1021/om030311t

Reference yield: 76.0%

: 609770-37-8
2-(Ph₃P=NCH₂)(C₅H₄N)

: 3375-31-3
palladium diacetate

: lithium chloride

: 1019321-70-0
[Pd(C6H4(PPh2=NCH2-C5H4N-2'-κ-C,N,N)-2)(Cl)]

Guidance literature:: In methanol; toluene; to soln. of a ligand (0.81 mmol) in toluene, Pd-contg. compd. (0.81 mmol) was added; mixt. was refluxed for 1 h; soln. was evapd. to dryness; residue in MeOH was treated with excess of LiCl (2.50 mmol); stirring for 3 h at 25°C; suspn. was filtered and solid was washed with MeOH and Et2O, dried by suction; elem. anal.;
DOI:10.1039/b714485g