C₃₆H₄₀ClNO₃Si

Base Information

Chemical Name:C₃₆H₄₀ClNO₃Si
CAS No.:951385-91-4
Molecular Formula:C₃₆H₄₀ClNO₃Si
Molecular Weight:598.257
Hs Code.:

C<sub>36</sub>H<sub>40</sub>ClNO<sub>3</sub>Si

Synonyms:C₃₆H₄₀ClNO₃Si

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Chemical Property of C₃₆H₄₀ClNO₃Si

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Technology Process of C₃₆H₄₀ClNO₃Si

There total 11 articles about C₃₆H₄₀ClNO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 951385-89-0
(R,E)-N-(6-chloro-1-(4-methoxyphenyl)-3-oxohex-4-en-2-yl)benzamide

: 951385-91-4
C₃₆H₄₀ClNO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1: lithium tri-tert-butoxyaluminohydride / ethanol; tetrahydrofuran / 2 h / -78 °C

2: 83 percent / triphenyl phosphine; diethyl azodicarboxylate; 4-nitrobenzoic acid / tetrahydrofuran; toluene / 0.25 h / 20 °C

3: 97 percent / aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

4: imidazole / dimethylformamide

With 1H-imidazole; hydrogenchloride; lithium tri(t-butoxy)aluminum hydride; triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene; 2: Mitsunobu reaction;
DOI:10.1021/ol701519b

Reference yield:

: 951385-88-9
(R)-N-(1-(methoxy(methyl)amino)-3-(4-methoxyphenyl)-1-oxopropan-2-yl)benzamide

: 951385-91-4
C₃₆H₄₀ClNO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: MeLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: 86 percent / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.1: lithium tri-tert-butoxyaluminohydride / ethanol; tetrahydrofuran / 2 h / -78 °C

3.1: 83 percent / triphenyl phosphine; diethyl azodicarboxylate; 4-nitrobenzoic acid / tetrahydrofuran; toluene / 0.25 h / 20 °C

4.1: 97 percent / aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

5.1: imidazole / dimethylformamide

With 1H-imidazole; hydrogenchloride; lithium tri(t-butoxy)aluminum hydride; methyllithium; triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; ethanol; hexane; N,N-dimethyl-formamide; toluene; 3.1: Mitsunobu reaction;
DOI:10.1021/ol701519b

Reference yield:

: 93634-70-9
(R)-4-methoxy-N-benzoyl-phenylalanine-methylester

: 951385-91-4
C₃₆H₄₀ClNO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: trimethylaluminum / CH₂Cl₂; hexane / 0.5 h / 20 °C

1.2: 98 percent / CH₂Cl₂; hexane / 1 h / 20 °C

2.1: MeLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 86 percent / tetrahydrofuran; hexane / 0.5 h / -78 °C

3.1: lithium tri-tert-butoxyaluminohydride / ethanol; tetrahydrofuran / 2 h / -78 °C

4.1: 83 percent / triphenyl phosphine; diethyl azodicarboxylate; 4-nitrobenzoic acid / tetrahydrofuran; toluene / 0.25 h / 20 °C

5.1: 97 percent / aq. HCl / tetrahydrofuran; methanol / 12 h / 20 °C

6.1: imidazole / dimethylformamide

With 1H-imidazole; hydrogenchloride; lithium tri(t-butoxy)aluminum hydride; methyllithium; trimethylaluminum; triphenylphosphine; diethylazodicarboxylate; 4-nitro-benzoic acid; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; toluene; 4.1: Mitsunobu reaction;
DOI:10.1021/ol701519b