methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

Base Information

Chemical Name:methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride
CAS No.:84638-99-3
Molecular Formula:C₂₅H₂₈N₂O₆*ClH
Molecular Weight:488.968
Hs Code.:

Synonyms:methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

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Chemical Property of methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

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Technology Process of methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

There total 7 articles about methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 84638-84-6
ethyl 7-hydroxy-1H-indole-2-carboxylate

: 84638-98-2
methyl 3-(N-benzyl-N-cyanomethyl)-aminobutyrate

: 84638-99-3
methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

Guidance literature:: With hydrogenchloride; aluminium trichloride; In 1,4-dioxane; at 5 - 10 ℃; for 16h;

Reference yield:

: 61535-21-5
1-(benzyloxy)-3-methyl-2-nitrobenzene

: 84638-99-3
methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / KOEt / diethyl ether / 20 h / Heating

2: 61 percent / iron powder / acetic acid / 3 h / 80 - 90 °C

3: 80 percent / hydrogen / Pd on carbon (10percent) / methanol; tetrahydrofuran / 12001 Torr

4: 72 percent / AlCl₃, HCl / dioxane / 16 h / 5 - 10 °C

With hydrogenchloride; aluminium trichloride; potassium ethoxide; hydrogen; iron; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; acetic acid;

Reference yield:

: 96564-49-7
ethyl 3-(3-benzyloxy-2-nitrophenyl)-pyruvate, potassium salt

: 84638-99-3
methyl-3-(N-<2-oxo-2-(2-ethoxycarbinol-7-hydroxyindole-4-yl)-ethyl>-N-benzylamino)-butyrate, hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / iron powder / acetic acid / 3 h / 80 - 90 °C

2: 80 percent / hydrogen / Pd on carbon (10percent) / methanol; tetrahydrofuran / 12001 Torr

3: 72 percent / AlCl₃, HCl / dioxane / 16 h / 5 - 10 °C

With hydrogenchloride; aluminium trichloride; hydrogen; iron; palladium on activated charcoal; In tetrahydrofuran; 1,4-dioxane; methanol; acetic acid;