(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

Base Information

Chemical Name:(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine
CAS No.:154742-98-0
Molecular Formula:C₃₆H₃₉N₇O₂
Molecular Weight:601.751
Hs Code.:

Synonyms:(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

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Chemical Property of (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

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Technology Process of (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

There total 2 articles about (3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 15496-36-3
bis[2-(2-pyridyl)ethyl]amine

: 51760-20-4
1,3-bis-bromomethyl-5-nitro-benzene

: 154742-98-0
(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

Guidance literature:: With triethylamine; In ethyl acetate; for 120h; Ambient temperature;
DOI:10.1021/ja00083a018

Reference yield:

: 99-12-7
5-nitro-m-xylene

: 154742-98-0
(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / NBS, dibenzoyl peroxide / CCl₄ / 24 h / Heating; Irradiation

2: 54 percent / Et₃N / ethyl acetate / 120 h / Ambient temperature

With N-Bromosuccinimide; triethylamine; dibenzoyl peroxide; In tetrachloromethane; ethyl acetate;
DOI:10.1021/ja00083a018

Reference yield: 64.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 154742-98-0
(3-{[Bis-(2-pyridin-2-yl-ethyl)-amino]-methyl}-5-nitro-benzyl)-bis-(2-pyridin-2-yl-ethyl)-amine

: Cu₂{C₆H₃(NO₂)(CH₂N(C₂H₄C₅H₄N)2)2}⁽²⁺⁾*2PF₆^(1-)={Cu₂{C₆H₃(NO₂)(CH₂N(C₂H₄C₅H₄N)2)2}}(PF₆)2

Guidance literature:: In dichloromethane; stirred for 0.5 h under Ar; pptd. with ether, liquid is decanted, solid is dissolved in CH2Cl2, filtd., pptd. with ether, liquid is decanted, solid is vacuum dried, elem. anal.;
DOI:10.1021/ja00083a018