N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Name:N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide
CAS No.:1402916-99-7
Molecular Formula:C₆₀H₄₆N₆O₄
Molecular Weight:915.063
Hs Code.:

Synonyms:N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

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Chemical Property of N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

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Technology Process of N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

There total 7 articles about N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 1402916-96-4
C₄₈H₄₄N₄O₄

: 1402916-99-7
N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: With trifluorormethanesulfonic acid; In N,N-dimethyl-formamide; at 110 ℃;
DOI:10.1016/j.tet.2012.08.084

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 1402916-99-7
N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid / chloroform / 5 h / 20 °C

1.2: 12 h / 140 °C / Inert atmosphere

2.1: 10% Pd/C; hydrazine / 1,2-dimethoxyethane / 0.25 h / 83 °C

3.1: trifluorormethanesulfonic acid / N,N-dimethyl-formamide / 110 °C

With trifluorormethanesulfonic acid; 10% Pd/C; nitric acid; hydrazine; In 1,2-dimethoxyethane; chloroform; N,N-dimethyl-formamide; 3.1: |Pictet-Spengler Synthesis;
DOI:10.1016/j.tet.2012.08.084

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1402916-99-7
N,N′-bis(2′,6′-diisopropylphenyl)-syn-13,14-di((pyridin-2″-yl)-azabenzo[pqr])-perylene-3,4:9,10-tetracarboxylic acid bisimide

Guidance literature:: Multi-step reaction with 3 steps

1.1: nitric acid / chloroform / 5 h / 20 °C

1.2: 12 h / 140 °C / Inert atmosphere

2.1: 10% Pd/C; hydrazine / 1,2-dimethoxyethane / 0.25 h / 83 °C

3.1: trifluorormethanesulfonic acid / N,N-dimethyl-formamide / 110 °C

With trifluorormethanesulfonic acid; 10% Pd/C; nitric acid; hydrazine; In 1,2-dimethoxyethane; chloroform; N,N-dimethyl-formamide; 3.1: |Pictet-Spengler Synthesis;
DOI:10.1016/j.tet.2012.08.084