(2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

Base Information

Chemical Name:(2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol
CAS No.:674769-28-9
Molecular Formula:C₁₄H₁₈O₅
Molecular Weight:266.294
Hs Code.:

Synonyms:(2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

Suppliers and Price of (2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

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Chemical Property of (2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

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Technology Process of (2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

There total 2 articles about (2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2873-29-2
D-glucal triacetate

: 674769-28-9
(2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / PPh₃*HBr / acetonitrile

2: Et₂NH

3: TsOH

With triphenylphosphine hydrobromide; toluene-4-sulfonic acid; diethylamine; In acetonitrile;
DOI:10.1021/ol036393z

Reference yield:

: 126873-07-2
methyl 3,4,6-tri-O-acetyl-2-deoxy-α/β-D-glucopyranoside

: 674769-28-9
(2S,4aR,8R,8aS)-6-Methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-ol

Guidance literature:: Multi-step reaction with 2 steps

1: Et₂NH

2: TsOH

With toluene-4-sulfonic acid; diethylamine;
DOI:10.1021/ol036393z