13-acetyl-7,10-dimethoxy-10-DAB

Base Information

Chemical Name:13-acetyl-7,10-dimethoxy-10-DAB
CAS No.:1402820-67-0
Molecular Formula:C₃₃H₄₂O₁₁
Molecular Weight:614.69
Hs Code.:

Synonyms:13-acetyl-7,10-dimethoxy-10-DAB

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Chemical Property of 13-acetyl-7,10-dimethoxy-10-DAB

Chemical Property:

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Technology Process of 13-acetyl-7,10-dimethoxy-10-DAB

There total 4 articles about 13-acetyl-7,10-dimethoxy-10-DAB which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1402820-66-9
13-acetyl-7,10-methylthiomethyl-10-DAB

: 1402820-67-0
13-acetyl-7,10-dimethoxy-10-DAB

Guidance literature:: With water; Raney nickel; In methanol; at 23 ℃;

Reference yield:

: 32981-86-5,172018-16-5
10-deacetylbaccatin III

: 1402820-67-0
13-acetyl-7,10-dimethoxy-10-DAB

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / pyridine / 20 h / 23 °C / Inert atmosphere

2: hydrazine hydrate / N,N-dimethyl-formamide / 20 h / 0 °C / Inert atmosphere

3: acetic anhydride; acetic acid / 120 h / 23 °C / Inert atmosphere

4: water / Raney nickel / methanol / 23 °C

With dmap; water; acetic anhydride; hydrazine hydrate; acetic acid; Raney nickel; In pyridine; methanol; N,N-dimethyl-formamide;

Reference yield:

: 92950-44-2
7,13-diacetyl baccatin III

: 1402820-67-0
13-acetyl-7,10-dimethoxy-10-DAB

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / N,N-dimethyl-formamide / 20 h / 0 °C / Inert atmosphere

2: acetic anhydride; acetic acid / 120 h / 23 °C / Inert atmosphere

3: water / Raney nickel / methanol / 23 °C

With water; acetic anhydride; hydrazine hydrate; acetic acid; Raney nickel; In methanol; N,N-dimethyl-formamide;