potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide

Base Information

• Chemical Name: potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide
• CAS No.: 80662-97-1
• Molecular Formula: C₁₈H₈F₁₂O₃S*2K
• Molecular Weight: 610.503
• Mol file: 80662-97-1.mol

Synonyms:potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide

Chemical Property of potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide

Chemical Property:

Purity/Quality:

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Technology Process of potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide

There total 1 articles about potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3,3,3',3'-Tetrakis(trifluoromethyl)-1,1'-spiro<3H-2,1-benzixathiole> (70091-68-8) → potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide (80662-97-1)

Guidance literature:

With potassium hydroxide; In ethanol; water; for 168h; Heating;

DOI:10.1021/ja00370a039

Reference yield: 73.0%

tetra(n-butyl)ammonium hydroxide (2052-49-5) + potassium salt of bis<2-(1,1,1,3,3,3-hexafluoro-2-hydroxypropyl)phenyl>sulfoxide (80662-97-1) → 1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium; (80662-99-3)

Guidance literature:

In water;

DOI:10.1021/ja00370a039

upstream raw materials:

3,3,3',3'-Tetrakis(trifluoromethyl)-1,1'-spiro<3H-2,1-benzixathiole>

Downstream raw materials:

1,1,1,3,3,3-Hexafluoro-2-{2-[2-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-benzenesulfinyl]-phenyl}-propan-2-olatetetrabutyl-ammonium;