Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Base Information

Chemical Name:Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester
CAS No.:143570-28-9
Molecular Formula:C₄₉H₅₉O₈PS
Molecular Weight:839.042
Hs Code.:

Synonyms:Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Suppliers and Price of Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

There total 3 articles about Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111-88-6
Octanethiol

: 143570-28-9
Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) n-BuLi / 1) THF, 0 deg C, 30 min, 2) room temp., 1 h

2: CH₂Cl₂ / 6 h / Ambient temperature

3: triisopropylbenzenesulfonyl chloride (TPSCl), NEt₃, pyridine / 24 h / Ambient temperature

With pyridine; n-butyllithium; triisopropylbenzenesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)74812-X

Reference yield:

: 20195-14-6
O,O-diethyl S-n-octane phosphorothioate

: 143570-28-9
Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 6 h / Ambient temperature

2: triisopropylbenzenesulfonyl chloride (TPSCl), NEt₃, pyridine / 24 h / Ambient temperature

With pyridine; triisopropylbenzenesulfonyl chloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)74812-X

Reference yield:

: 6195-45-5,13264-84-1,22132-86-1,25018-91-1,26277-05-4,28366-79-2,30694-52-1
DL-2,3,4,5,6-penta-O-benzyl-myo-inositol

: C₁₄H₃₅O₃PSSi₂

: 143570-28-9
Thiophosphoric acid S-octyl ester O-((1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl) ester

Guidance literature:: With pyridine; triisopropylbenzenesulfonyl chloride; triethylamine; for 24h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4039(00)74812-X