Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

Base Information

Chemical Name:Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride
CAS No.:125424-05-7
Molecular Formula:C₁₂H₂₃NO₂*ClH
Molecular Weight:249.781
Hs Code.:

Synonyms:Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

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Chemical Property of Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

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Technology Process of Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

There total 5 articles about Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 120143-37-5
(1S,3S,4R)-menthyl glycinate

: 125424-05-7
Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In diethyl ether; for 2h;
DOI:10.1016/S0040-4039(00)94713-0

Reference yield:

: 2216-51-5
(-)-menthol

: 125424-05-7
Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / N,N-diethylaniline / diethyl ether / Heating

2: 91 percent / NaN₃ / acetone; H₂O / Heating

3: 95 percent / hydrogen / Pd/BaSO₄ / methanol

4: 92 percent / HCl (gas) / diethyl ether / 2 h

With hydrogenchloride; sodium azide; hydrogen; N,N-diethylaniline; Pd-BaSO₄; In methanol; diethyl ether; water; acetone;
DOI:10.1016/S0040-4039(00)94713-0

Reference yield:

: Azido-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester

: 125424-05-7
Amino-acetic acid (1S,2R,5S)-2-isopropyl-5-methyl-cyclohexyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / hydrogen / Pd/BaSO₄ / methanol

2: 92 percent / HCl (gas) / diethyl ether / 2 h

With hydrogenchloride; hydrogen; Pd-BaSO₄; In methanol; diethyl ether;
DOI:10.1016/S0040-4039(00)94713-0