2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

Base Information

Chemical Name:2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid
CAS No.:1360822-11-2
Molecular Formula:C₂HF₃O₂*C₁₃H₁₈N₂O₅
Molecular Weight:396.32
Hs Code.:

Synonyms:2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

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Chemical Property of 2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

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Technology Process of 2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

There total 7 articles about 2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1360822-09-8
2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

: 76-05-1
trifluoroacetic acid

: 1360822-11-2
2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

Guidance literature:: In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 448-19-1
4-fluoro-2-methoxy-1-nitrobenzene

: 1360822-11-2
2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 20 h / 80 °C

1.2: pH 5

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 70 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

4.1: pyridine / tetrahydrofuran / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 0.5 h / 2585.81 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C

7.1: dichloromethane / 1 h / 20 °C

With pyridine; hydrogenchloride; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 16292-95-8
4-nitro-3-methoxyphenol

: 1360822-11-2
2-(4-(2-aminoacetamido)-3-methoxyphenoxy)ethyl acetate trifluoroacetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 70 °C

2: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

3: pyridine / tetrahydrofuran / 0 - 20 °C

4: hydrogen / palladium 10% on activated carbon / ethyl acetate / 0.5 h / 2585.81 Torr

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C

6: dichloromethane / 1 h / 20 °C

With pyridine; hydrogenchloride; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;