2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

Base Information

Chemical Name:2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate
CAS No.:1360822-09-8
Molecular Formula:C₁₈H₂₆N₂O₇
Molecular Weight:382.414
Hs Code.:

Synonyms:2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

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Chemical Property of 2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

Chemical Property:

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Technology Process of 2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

There total 6 articles about 2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 4530-20-5
BOC-glycine

: 1360822-08-7
acetic acid 2-(4-amino-3-methoxy-phenoxy)-ethyl ester

: 1360822-09-8
2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: 448-19-1
4-fluoro-2-methoxy-1-nitrobenzene

: 1360822-09-8
2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydroxide / dimethyl sulfoxide / 20 h / 80 °C

1.2: pH 5

2.1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 70 °C

3.1: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

4.1: pyridine / tetrahydrofuran / 0 - 20 °C

5.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 0.5 h / 2585.81 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C

With pyridine; hydrogenchloride; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 16292-95-8
4-nitro-3-methoxyphenol

: 1360822-09-8
2-(4-(2-(tert-butoxycarbonylamino)acetamido)-3-methoxyphenoxy)ethyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 h / 70 °C

2: hydrogenchloride / tetrahydrofuran; water / 1 h / 20 °C

3: pyridine / tetrahydrofuran / 0 - 20 °C

4: hydrogen / palladium 10% on activated carbon / ethyl acetate / 0.5 h / 2585.81 Torr

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 h / 20 °C

With pyridine; hydrogenchloride; hydrogen; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;