(1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

Base Information

Chemical Name:(1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane
CAS No.:753488-83-4
Molecular Formula:C₁₆H₃₀O
Molecular Weight:238.414
Hs Code.:

Synonyms:(1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

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Technology Process of (1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

There total 4 articles about (1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2216-51-5
(-)-menthol

: 753488-83-4
(1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

Guidance literature:: (-)-menthol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 1h;

Me₂C=C(Me)CH₂-X; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/ol049135q

Reference yield:

: 2216-51-5
(-)-menthol

: 753488-83-4
(1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / tetrahydrofuran / 1 h / 0 °C

1.2: 86.2 percent / tetrahydrofuran / 0 °C

2.1: (PhSO₂)2 / toluene; CD₂Cl₂ / 120 h / 80 °C

2.2: H₂O / 80 °C

3.1: NaH / tetrahydrofuran / 1 h / 0 °C

3.2: 82 percent / tetrahydrofuran / 0 °C

With (PhSO₂)2; sodium hydride; In tetrahydrofuran; dichloromethane-d2; toluene;
DOI:10.1021/ol049135q

Reference yield:

: 180477-54-7
(1S,2R,4R)-1-isopropyl-4-methyl-2-(3-methylbut-2-en-1-yloxy)cyclohexane

: 753488-83-4
(1S,2R,4R)-2-(2,3-dimethylbut-2-en-1-yloxy)-1-isopropyl-4-methylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: (PhSO₂)2 / toluene; CD₂Cl₂ / 21 h / 80 °C

2.1: NaH / tetrahydrofuran / 1 h / 0 °C

2.2: 82 percent / tetrahydrofuran / 0 °C

With (PhSO₂)2; sodium hydride; In tetrahydrofuran; dichloromethane-d2; toluene;
DOI:10.1021/ol049135q