1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

Base Information

Chemical Name:1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane
CAS No.:936576-76-0
Molecular Formula:C₃₆H₄₀N₂O₄S₂
Molecular Weight:628.857
Hs Code.:

Synonyms:1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

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Technology Process of 1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

There total 2 articles about 1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 936576-75-9
1-amino-2-[2,3-di(isopropylmercapto)benzamido]ethane

: 69146-58-3
2,3-bis(benzyloxy)benzoyl chloride

: 936576-76-0
1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/chem.200601167

Reference yield:

: 936576-74-8
1-(tert-butyloxycarbamido)-2-[2,3-di(isopropylmercapto)benzamido]ethane

: 936576-76-0
1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / trifluoroacetic acid / CHCl₃ / 24 h / 20 °C

2: 81 percent / NEt₃ / tetrahydrofuran / 12 h / 20 °C

With triethylamine; trifluoroacetic acid; In tetrahydrofuran; chloroform;
DOI:10.1002/chem.200601167

Reference yield: 91.0%

: 936576-76-0
1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane

: 1-(2,3-dihydroxybenzamido)-2-(2,3-dimercaptobenzamido)ethane

Guidance literature:: 1-[2,3-di(benzyloxy)benzamido]-2-[2,3-di(isopropylmercapto)benzamido]ethane; With naphthalene; sodium; In tetrahydrofuran; at 20 ℃; for 12h;

With hydrogenchloride; Further stages.;
DOI:10.1002/chem.200601167