4-hydroxy-4'-methoxytetraphenylmethane

Base Information

• Chemical Name: 4-hydroxy-4'-methoxytetraphenylmethane
• CAS No.: 615575-22-9
• Molecular Formula: C₂₆H₂₂O₂
• Molecular Weight: 366.459
• Mol file: 615575-22-9.mol

Synonyms:4-hydroxy-4'-methoxytetraphenylmethane

Chemical Property of 4-hydroxy-4'-methoxytetraphenylmethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-hydroxy-4'-methoxytetraphenylmethane

There total 4 articles about 4-hydroxy-4'-methoxytetraphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

mono-4-methoxytrityl chloride (14470-28-1) + phenol (108-95-2,27073-41-2) → 4-hydroxy-4'-methoxytetraphenylmethane (615575-22-9)

Guidance literature:

at 60 ℃; for 20h;

DOI:10.1021/ma034521t

Reference yield:

Dichlorodiphenylmethane (2051-90-3) → 4-hydroxy-4'-methoxytetraphenylmethane (615575-22-9)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃; CS₂

2: HCl

With hydrogenchloride; carbon disulfide; aluminium trichloride;

DOI:10.1039/jr9550003089

Reference yield:

methoxybenzene (100-66-3) → 4-hydroxy-4'-methoxytetraphenylmethane (615575-22-9)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃; CS₂

2: HCl

With hydrogenchloride; carbon disulfide; aluminium trichloride;

DOI:10.1039/jr9550003089

upstream raw materials:

mono-4-methoxytrityl chloride

phenol

p-methoxytrityl alcohol

Dichlorodiphenylmethane

Downstream raw materials:

4-(diphenyl-tert-butylsiloxy)-4'-hydroxytetraphenylmethane

bisphenol TP

Refernces

• 1、 Werts, Michel P.L.,Van Den Boogaard, Maarten,Tsivgoulis, Gerasimos M.,Hadziioannou, George. "Mechanically linked polyrotaxanes: A stepwise approach". . p. 7004 - 7013. Retrieved 2007/10/03.