Technology Process of L-Norvaline,N-[(1,1-dimethylethoxy)carbonyl]-N-methyl-
There total 6 articles about L-Norvaline,N-[(1,1-dimethylethoxy)carbonyl]-N-methyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / ammonium formate / 10percent Pd/C / methanol / 4 h / Ambient temperature
2: 1 N NaOH / dioxane
With
sodium hydroxide; ammonium formate;
palladium on activated charcoal;
In
1,4-dioxane; methanol;
DOI:10.1016/0040-4020(96)00242-6
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylsilane, TFA / CH2Cl2 / 20 h / Ambient temperature
2: 100 percent / ammonium formate / 10percent Pd/C / methanol / 4 h / Ambient temperature
3: 1 N NaOH / dioxane
With
triethylsilane; sodium hydroxide; ammonium formate; trifluoroacetic acid;
palladium on activated charcoal;
In
1,4-dioxane; methanol; dichloromethane;
DOI:10.1016/0040-4020(96)00242-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: triethylamine / dioxane; H2O / 4 h / Ambient temperature
2: NaH / tetrahydrofuran / 24 h / Ambient temperature
With
sodium hydride; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1016/S0040-4020(01)80978-9