N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

Base Information

Chemical Name:N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline
CAS No.:342632-58-0
Molecular Formula:C₁₈H₁₇Cl₂N₅O
Molecular Weight:390.272
Hs Code.:

Synonyms:N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

Suppliers and Price of N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

There total 2 articles about N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 245539-10-0
1-isocyano-2,5-dichlorobenzene

: 342632-58-0
N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

Guidance literature:: morpholine; 1,2,3-Benzotriazole; formaldehyd; In water;

1-isocyano-2,5-dichlorobenzene; With boron trifluoride diethyl etherate; In tetrahydrofuran; at 25 ℃; Further stages.;
DOI:10.1021/jo0016935

Reference yield:

: 6639-55-0
N-(2,5-dichlorophenyl)formamide

: 342632-58-0
N-[1-(1H-benzotriazol-1-yl)-2-morpholinoethylidene]-2,5-dichloroaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: POCl₃; i-Pr₂NH / CH₂Cl₂ / 1 h / -10 °C

2.1: H₂O

2.2: BF₃*Et₂O / tetrahydrofuran / 25 °C

With diisopropylamine; trichlorophosphate; In dichloromethane; water;
DOI:10.1021/jo0016935