(1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

Base Information

Chemical Name:(1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine
CAS No.:211746-22-4
Molecular Formula:C₂₈H₃₁NO₃
Molecular Weight:429.559
Hs Code.:

Synonyms:(1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

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Chemical Property of (1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

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Technology Process of (1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

There total 5 articles about (1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 211746-21-3
(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

: 211746-22-4
(1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; for 12h; Ambient temperature;
DOI:10.1016/S0040-4020(98)00471-2

Reference yield:

: 34638-25-0,38110-77-9,43119-28-4,54483-22-6,26054-46-6
(1R,5S)-2-oxabicyclo[3.3.0]oct-6-en-3-one

: 211746-22-4
(1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

Guidance literature:: Multi-step reaction with 5 steps

1.1: DIBAL-H

2.1: Et₃N

3.1: Et₃N

4.1: NaN₃ / dimethylformamide

5.1: PPh₃ / tetrahydrofuran

5.2: H₂O

With sodium azide; diisobutylaluminium hydride; triethylamine; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Reduction / 2.1: Substitution / 3.1: Substitution / 4.1: Substitution / 5.1: Addition / 5.2: Hydrolysis;
DOI:10.1080/15257779908041509

Reference yield:

: 54483-54-4
(+)-2β-hydroxyethyl-3-cyclopenten-1β-ol

: 211746-22-4
(1S,2S)-2-{2-[Bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enylamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: Et₃N

2.1: Et₃N

3.1: NaN₃ / dimethylformamide

4.1: PPh₃ / tetrahydrofuran

4.2: H₂O

With sodium azide; triethylamine; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; 1.1: Substitution / 2.1: Substitution / 3.1: Substitution / 4.1: Addition / 4.2: Hydrolysis;
DOI:10.1080/15257779908041509