(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

Base Information

Chemical Name:(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether
CAS No.:211746-21-3
Molecular Formula:C₂₈H₂₉N₃O₃
Molecular Weight:455.557
Hs Code.:

Synonyms:(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

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Chemical Property of (1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

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Technology Process of (1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

There total 4 articles about (1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 211746-20-2
Methanesulfonic acid (1R,2S)-2-{2-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-ethyl}-cyclopent-3-enyl ester

: 211746-21-3
(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 75 ℃; for 10h;
DOI:10.1016/S0040-4020(98)00471-2

Reference yield:

: 34638-25-0,38110-77-9,43119-28-4,54483-22-6,26054-46-6
(1R,5S)-2-oxabicyclo[3.3.0]oct-6-en-3-one

: 211746-21-3
(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: DIBAL-H

2: Et₃N

3: Et₃N

4: NaN₃ / dimethylformamide

With sodium azide; diisobutylaluminium hydride; triethylamine; In N,N-dimethyl-formamide; 1: Reduction / 2: Substitution / 3: Substitution / 4: Substitution;
DOI:10.1080/15257779908041509

Reference yield:

: 54483-54-4
(+)-2β-hydroxyethyl-3-cyclopenten-1β-ol

: 211746-21-3
(1S,2S)-2-(2-azidocyclopent-4-enyl)ethanol (4,4'-dimethoxy)triphenylmethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N

2: Et₃N

3: NaN₃ / dimethylformamide

With sodium azide; triethylamine; In N,N-dimethyl-formamide; 1: Substitution / 2: Substitution / 3: Substitution;
DOI:10.1080/15257779908041509