(R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

Base Information

Chemical Name:(R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)
CAS No.:1346531-02-9
Molecular Formula:C₄₁H₄₈O₁₅
Molecular Weight:780.823
Hs Code.:

Synonyms:(R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

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Technology Process of (R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

There total 1 articles about (R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1034343-24-2
4-O-benzyl-3,5-di-O-(methoxymethyl)gallic acid

: 130408-40-1
(R)-2-methoxy-1,4-butanediol

: 1346531-02-9
(R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo201750d

Reference yield: 99.0%

: 1346531-02-9
(R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

: 1346531-07-4
(R)-2-methoxy-1,4-butandiyl bis(4-O-benzylgallate)

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; isopropyl alcohol; at 60 ℃; for 21h;
DOI:10.1021/jo201750d

Reference yield:

: 1346531-02-9
(R)-2-methoxy-1,4-butandiyl bis(4-O-benzyl-3,5-di-O-(methoxymethyl)gallate)

: (R)-2-methoxy-1,4-butandiyl 5,5'-bis(benzyloxy)-4,4',6,6'-tetrahydroxy-1,1'-biphenyl-2,2'-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / tetrahydrofuran; water; isopropyl alcohol / 21 h / 60 °C

2: N-butylamine; copper dichloride / methanol / 0.5 h / 20 °C

With hydrogenchloride; N-butylamine; copper dichloride; In tetrahydrofuran; methanol; water; isopropyl alcohol;
DOI:10.1021/jo201750d