4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

Base Information

Chemical Name:4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester
CAS No.:1287116-19-1
Molecular Formula:C₁₇H₁₅ClN₂O₅
Molecular Weight:362.769
Hs Code.:

Synonyms:4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

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Chemical Property of 4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

Chemical Property:

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Technology Process of 4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

There total 3 articles about 4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 33977-11-6
5-chloro-2-methoxybenzoylhydrazide

: 7377-26-6
4-Methoxycarbonylbenzoyl chloride

: 1287116-19-1
4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

Guidance literature:: With pyridine; In tetrahydrofuran; for 4h; Cooling with ice; Heating;
DOI:10.1016/j.tetlet.2012.12.128

Reference yield:

: 68216-06-8
ethyl 5-chloro-2-methoxybenzoate

: 1287116-19-1
4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 24 h / Reflux; Inert atmosphere

2: tetrahydrofuran / 1 h / Cooling

With hydrazine hydrate; In tetrahydrofuran; ethanol;

Reference yield:

: 3438-16-2
5-chloro-2-methoxybenzoic acid

: 1287116-19-1
4-(2-(5-chloro-2-methoxyphenyl)carbohydrazide)benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 24 h / Reflux

2: hydrazine hydrate / ethanol / 24 h / Reflux; Inert atmosphere

3: tetrahydrofuran / 1 h / Cooling

With sulfuric acid; hydrazine hydrate; In tetrahydrofuran; ethanol;