1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline

Base Information

Chemical Name:1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline
CAS No.:203522-45-6
Molecular Formula:C₂₄H₂₆N₂O₇
Molecular Weight:454.48
Hs Code.:

Synonyms:1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline

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Chemical Property of 1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline

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Technology Process of 1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline

There total 2 articles about 1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 108-30-5
succinic acid anhydride

: 148318-12-1
3-amino-1-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline

: 203522-45-6
1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline

Guidance literature:: In 1,4-dioxane; for 0.5h; Heating;
DOI:10.1007/BF02464152

Reference yield:

: 172421-62-4
3-acetylamino-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline

: 203522-45-6
1-(3,4-dimethoxybenzyl)-3-carboxypropionylglycilamino-6,7-dimethoxyisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 25 percent KOH / ethanol / 1 h / Heating

2: 98 percent / dioxane / 0.5 h / Heating

With potassium hydroxide; In 1,4-dioxane; ethanol; 1: Hydrolysis / 2: Acylation;
DOI:10.1007/BF02464152