methyl 2,4-dinitro-5-benzoate

Base Information

Chemical Name:methyl 2,4-dinitro-5-benzoate
CAS No.:156423-06-2
Molecular Formula:C₁₂H₁₅N₃O₇
Molecular Weight:313.267
Hs Code.:

methyl 2,4-dinitro-5-<N-(2-hydroxyethyl)-N-ethylamino>benzoate

Synonyms:methyl 2,4-dinitro-5-benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2,4-dinitro-5-benzoate

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Technology Process of methyl 2,4-dinitro-5-benzoate

There total 1 articles about methyl 2,4-dinitro-5-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 150272-08-5
methyl 5-chloro-2,4-dinitrobenzoate

: 110-73-6
2-(Ethylamino)ethanol

: 156423-06-2
methyl 2,4-dinitro-5-benzoate

Guidance literature:: In 1,4-dioxane; at 20 ℃; for 8h;
DOI:10.1021/jm00040a009

Reference yield:

: 124-63-0
methanesulfonyl chloride

: 156423-06-2
methyl 2,4-dinitro-5-benzoate

: 1027283-98-2
5-[Ethyl-(2-methanesulfonyloxy-ethyl)-amino]-2,4-dinitro-benzoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jm00040a009

Reference yield:

: 156423-06-2
methyl 2,4-dinitro-5-benzoate

: 156423-08-4
5--2,4-dinitrobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

2: LiCl / dimethylformamide / 0.25 h / 80 °C

3: 88 percent / aq. NaOH / methanol / 1 h / Heating

With sodium hydroxide; triethylamine; lithium chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00040a009