butyrophenone (E)-benzoylhydrazone

Base Information

• Chemical Name: butyrophenone (E)-benzoylhydrazone
• CAS No.: 372960-23-1
• Molecular Formula: C₁₇H₁₈N₂O
• Molecular Weight: 266.343
• Mol file: 372960-23-1.mol

Synonyms:butyrophenone (E)-benzoylhydrazone

Chemical Property of butyrophenone (E)-benzoylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of butyrophenone (E)-benzoylhydrazone

There total 1 articles about butyrophenone (E)-benzoylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoic acid hydrazide (613-94-5) + propiophenone (495-40-9) → butyrophenone (E)-benzoylhydrazone (372960-23-1)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 8h;

DOI:10.1021/jo0258599

Reference yield: 87.0%

allyltrichlorosilane (107-37-9) + butyrophenone (E)-benzoylhydrazone (372960-23-1) → N'-(1-phenyl-1-propyl-3-butenyl)benzohydrazide

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 3h;

DOI:10.1021/ja011125m

Reference yield:

butyrophenone (E)-benzoylhydrazone (372960-23-1) → 2-methyl-1-phenyl-1-propylbut-3-enylamine

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide / 24 h / 20 °C

2: 49 percent / SmI₂ / methanol; tetrahydrofuran / 24 h / -78 °C

With samarium diiodide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1021/jo0258599

upstream raw materials:

benzoic acid hydrazide

propiophenone