C₂₀H₂₇ClF₃NO₄S

Base Information

Chemical Name:C₂₀H₂₇ClF₃NO₄S
CAS No.:1599479-15-8
Molecular Formula:C₂₀H₂₇ClF₃NO₄S
Molecular Weight:469.953
Hs Code.:

C<sub>20</sub>H<sub>27</sub>ClF<sub>3</sub>NO<sub>4</sub>S

Synonyms:C₂₀H₂₇ClF₃NO₄S

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Chemical Property of C₂₀H₂₇ClF₃NO₄S

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Technology Process of C₂₀H₂₇ClF₃NO₄S

There total 8 articles about C₂₀H₂₇ClF₃NO₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1599478-33-7
C₁₉H₂₅ClF₃NO₂

: 124-63-0
methanesulfonyl chloride

: 1599479-15-8
C₂₀H₂₇ClF₃NO₄S

Guidance literature:: With triethylamine; In dichloromethane; at -10 ℃; for 1h; Inert atmosphere;

Reference yield:

: 1599478-96-2
benzyl 9-(2-methoxy-2-oxoethylidene)-3-azaspiro[5.5]undec-7-ene-3-carboxylate

: 1599479-15-8
C₂₀H₂₇ClF₃NO₄S

Guidance literature:: Multi-step reaction with 6 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 35 - 40 °C / 2585.81 Torr

2: methanol; hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

3: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate / 1,4-dioxane / 36 h / 100 °C / Inert atmosphere

4: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C

5: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6: triethylamine / dichloromethane / 1 h / -10 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; methanol; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; borane-THF; palladium 10% on activated carbon; water; hydrogen; caesium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 138163-08-3
N-(benzyloxycarbonyl)piperidine-4-carboxaldehyde

: 1599479-15-8
C₂₀H₂₇ClF₃NO₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: potassium tert-butylate / tert-butyl methyl ether; isopropyl alcohol / 2 h / 10 - 30 °C

2.1: sodium hydride / tetrahydrofuran / 1.5 h / 0 - 30 °C / Inert atmosphere

2.2: 40 - 50 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 35 - 40 °C / 2585.81 Torr

4.1: methanol; hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

5.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; caesium carbonate / 1,4-dioxane / 36 h / 100 °C / Inert atmosphere

6.1: water; lithium hydroxide / tetrahydrofuran; methanol / 20 °C

7.1: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 1 h / -10 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; methanol; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; borane-THF; palladium 10% on activated carbon; potassium tert-butylate; water; hydrogen; sodium hydride; caesium carbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; tert-butyl methyl ether; isopropyl alcohol;