lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

Base Information

Chemical Name:lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate
CAS No.:1349833-44-8
Molecular Formula:C₃₉H₄₈NO₁₁*Li
Molecular Weight:713.751
Hs Code.:

lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

Synonyms:lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

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Chemical Property of lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

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Technology Process of lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

There total 7 articles about lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1349833-43-7
methyl (2S,3S,4S,5R,6S)-3,4,5-triacetoxy-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)tetrahydro-2H-pyran-2-carboxylate

: 1349833-44-8
lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; methanol; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo2018763

Reference yield:

: 60-12-8
2-phenylethanol

: 1349833-44-8
lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,1,1,3,3,3-hexamethyl-disilazane / 25 °C / Inert atmosphere

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -78 - 25 °C / Molecular sieve; Inert atmosphere

3: water; lithium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; water; 1,1,1,3,3,3-hexamethyl-disilazane; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo2018763

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1349833-44-8
lithium (2S,3S,4S,5R,6S)-6-(4-((4-((3,7-dimethyloct-6-enyloxy)(phenethoxy)methyl)phenylcarbamoyloxy)-methyl)phenoxy)-3,4,5-trihydroxytetrahydro-2H-pyran-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: silver(l) oxide / acetonitrile / 18 h / 25 °C / Inert atmosphere; Darkness

2.1: sodium tetrahydroborate / methanol; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0 - 25 °C / Inert atmosphere

3.2: 0 - 5 °C / Inert atmosphere

4.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -78 - 25 °C / Molecular sieve; Inert atmosphere

5.1: water; lithium hydroxide / tetrahydrofuran; methanol / 1 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; oxalyl dichloride; trimethylsilyl trifluoromethanesulfonate; water; silver(l) oxide; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo2018763