3-methyl-dodecane-1,3-diol

Base Information

• Chemical Name: 3-methyl-dodecane-1,3-diol
• CAS No.: 857786-65-3
• Molecular Formula: C₁₃H₂₈O₂
• Molecular Weight: 216.364
• Mol file: 857786-65-3.mol

Synonyms:3-methyl-dodecane-1,3-diol

Chemical Property of 3-methyl-dodecane-1,3-diol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-methyl-dodecane-1,3-diol

There total 1 articles about 3-methyl-dodecane-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3-epoxy-3-methyl-dodecanoic acid ethyl ester (83803-54-7) + ethanol (64-17-5) → 3-methyl-dodecane-1,3-diol (857786-65-3) + undecan-2-ol (1653-30-1,113666-64-1) + methyl nonyl ketone (112-12-9)

Guidance literature:

Reference yield:

3-methyl-dodecane-1,3-diol (857786-65-3) → 3-dodecanone (1534-27-6)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid anhydride; sodium acetate / und folgendes Verseifen

2: bei der Ozonspaltung

3: NaHSO₄ / folgende Hydrierung an Nickel in Aethanol und Behandlung mit CrO₃ in Eisessig

With sodium hydrogen sulfate; sodium acetate; acetic anhydride;

DOI:10.1002/hlca.193201501142

Reference yield:

3-methyl-dodecane-1,3-diol (857786-65-3) → diphenyl-carbamic acid-(3-nonyl-but-3-enyl ester)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid anhydride; sodium acetate / und folgendes Verseifen

2: pyridine

With pyridine; sodium acetate; acetic anhydride;

DOI:10.1002/hlca.193201501142

upstream raw materials:

2,3-epoxy-3-methyl-dodecanoic acid ethyl ester

ethanol

Downstream raw materials:

3-dodecanone