ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

Base Information

Chemical Name:ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid
CAS No.:1313053-26-7
Molecular Formula:C₂₅H₂₉BO₅
Molecular Weight:420.313
Hs Code.:

Synonyms:ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

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Chemical Property of ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

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Technology Process of ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

There total 5 articles about ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 5419-55-6
Triisopropyl borate

: 1313053-25-6
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

: 1313053-26-7
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

Guidance literature:: ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.25h; Inert atmosphere;

Triisopropyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; hexane;

Reference yield:

: 20098-14-0
chemantane

: 1313053-26-7
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanesulfonic acid / dichloromethane / 5 h / 80 °C

2.1: potassium carbonate / acetone / 25.7 h / Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid / benzene / 24.25 h / 110 °C / Dean-Stark apparatus

4.1: n-butyllithium / hexane; tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

With n-butyllithium; methanesulfonic acid; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; dichloromethane; acetone; benzene;

Reference yield:

: 106-41-2
4-bromo-phenol

: 1313053-26-7
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenylboronic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanesulfonic acid / dichloromethane / 5 h / 80 °C

2.1: potassium carbonate / acetone / 25.7 h / Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid / benzene / 24.25 h / 110 °C / Dean-Stark apparatus

4.1: n-butyllithium / hexane; tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

With n-butyllithium; methanesulfonic acid; potassium carbonate; toluene-4-sulfonic acid; In tetrahydrofuran; hexane; dichloromethane; acetone; benzene;