ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

Base Information

Chemical Name:ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide
CAS No.:1313053-25-6
Molecular Formula:C₂₅H₂₇BrO₃
Molecular Weight:455.392
Hs Code.:

Synonyms:ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

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Chemical Property of ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

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Technology Process of ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

There total 4 articles about ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1313053-24-5
5-(2'-benzyloxy-5'-bromophenyl)-2-adamantanone

: 107-21-1
ethylene glycol

: 1313053-25-6
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 110 ℃; for 24.25h; Dean-Stark apparatus;

Reference yield:

: 20098-14-0
chemantane

: 1313053-25-6
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonic acid / dichloromethane / 5 h / 80 °C

2: potassium carbonate / acetone / 25.7 h / Reflux; Inert atmosphere

3: toluene-4-sulfonic acid / benzene / 24.25 h / 110 °C / Dean-Stark apparatus

With methanesulfonic acid; potassium carbonate; toluene-4-sulfonic acid; In dichloromethane; acetone; benzene;

Reference yield:

: 106-41-2
4-bromo-phenol

: 1313053-25-6
ethyleneglycol ketal of 4-benzyloxy-3-[1-(4-oxoadamantyl)]phenyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: methanesulfonic acid / dichloromethane / 5 h / 80 °C

2: potassium carbonate / acetone / 25.7 h / Reflux; Inert atmosphere

3: toluene-4-sulfonic acid / benzene / 24.25 h / 110 °C / Dean-Stark apparatus

With methanesulfonic acid; potassium carbonate; toluene-4-sulfonic acid; In dichloromethane; acetone; benzene;