(1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Base Information

Chemical Name:(1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide
CAS No.:127126-09-4
Molecular Formula:C₁₉H₃₉NO₄Si
Molecular Weight:373.608
Hs Code.:

Synonyms:(1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

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Chemical Property of (1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

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Technology Process of (1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

There total 11 articles about (1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 127126-09-4
(1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 3 steps

1: 2,6-lutidine / CH₂Cl₂ / 0 °C

2: toluene

3: 2,6-di-t-butyl-4-methyl pyridine / CH₂Cl₂ / 24 h / 22 - 24 °C

With 2,6-dimethylpyridine; 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; toluene;
DOI:10.1016/S0040-4039(00)80074-X

Reference yield:

: 116386-60-8
(1R,3R,4R)-3-Hydroxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

: 333-27-7
methyl trifluoromethanesulfonate

: 126788-77-0,127126-09-4
(1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃;
DOI:10.1021/ja00164a023

Reference yield:

: 4771-80-6
1,2,5,6-tetrahydrobenzoic acid

: 126788-77-0,127126-09-4
(1R,3R,4R)-3-Methoxy-4-triisopropylsilanyloxy-cyclohexanecarboxylic acid methoxy-methyl-amide

Guidance literature:: Multi-step reaction with 5 steps

1: m-CPBA / CH₂Cl₂ / 0 °C

2: chlorobenzene / 130 °C

3: 2,6-lutidine / CH₂Cl₂ / 0 °C

4: Al(CH₃)3 / toluene / 20 °C

5: 2,6-di-tert-butyl-4-methylpyridine / CH₂Cl₂ / 20 °C

With 2,6-dimethylpyridine; 2,6-di-tert-butyl-4-methylpyridine; trimethylaluminum; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chlorobenzene; toluene;
DOI:10.1021/ja00164a023