N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

Base Information

Chemical Name:N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester
CAS No.:203873-71-6
Molecular Formula:C₂₇H₃₄N₂O₅
Molecular Weight:466.577
Hs Code.:

Synonyms:N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

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Chemical Property of N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

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Technology Process of N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

There total 10 articles about N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 133010-06-7
1,1-dimethylethyl S-N-(1-fluorocarbonyl-2-phenylethyl)carbamate

: 73270-67-4
(S)-2-allylamino-3-phenyl-propionic acid methyl ester

: 203873-71-6
N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

Guidance literature:: With N-ethylmorpholine;; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/jo991649t

Reference yield: 75.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 73270-67-4
(S)-2-allylamino-3-phenyl-propionic acid methyl ester

: 203873-71-6
N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

Guidance literature:: With N-Ethylmaleimide; In dichloromethane;
DOI:10.1016/S0960-894X(98)00289-3

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 203873-71-6
N-allyl-tert-butyloxycarbonyl-L-phenylalaninyl-L-phenylalanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / cyanuric fluoride; pyridine / CH₂Cl₂ / 1 h / -15 °C

2: 75 percent / N-ethylmorpholine / CH₂Cl₂ / 48 h / 20 °C

With N-ethylmorpholine;; pyridine; trifluoro-[1,3,5]triazine; In dichloromethane; 1: Fluorination / 2: Acylation;
DOI:10.1021/jo991649t