1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione

Base Information

• Chemical Name: 1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione
• CAS No.: 121400-87-1
• Molecular Formula: C₂₄H₁₈N₄O₄
• Molecular Weight: 426.431

Synonyms:1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione

Chemical Property of 1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione

Chemical Property:

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Technology Process of 1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione

There total 2 articles about 1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1,4-bis(phenylglyoxalyl)benzene (3363-97-1) + urea (57-13-6) → 1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione (121400-87-1)

Guidance literature:

In formic acid; water; at 130 ℃; for 1h;

Reference yield: 43.6%

1,4-bis(phenylglyoxalyl)benzene (3363-97-1) + 1,1'-phenylmethanediyl-bis-urea (23865-30-7) → 1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione (121400-87-1)

Guidance literature:

With sulfuric acid; acetic acid; for 10h; Heating;

Reference yield: 96.0%

1-phenyl-5-<4-(2-phenyl-1,2-dioxoethyl)phenyl>-2,4,6,8-tetraazabicyclo<3.3.0>octane-3,7-dione (121400-87-1) + urea (57-13-6) → 1,4-bis(5-phenyl-2,4,6,8-tetraaza-3,7-dioxobicyclo<3.3.0>octan-1-yl)benzene (121400-84-8)

Guidance literature:

In formic acid; at 125 ℃; for 0.333333h;

upstream raw materials:

1,4-bis(phenylglyoxalyl)benzene

urea

1,1'-phenylmethanediyl-bis-urea

Downstream raw materials:

1,4-bis(5-phenyl-2,4,6,8-tetraaza-3,7-dioxobicyclo<3.3.0>octan-1-yl)benzene

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