2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone

Base Information

• Chemical Name: 2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone
• CAS No.: 1130608-96-6
• Molecular Formula: C₂₀H₂₆N₂O₄
• Molecular Weight: 358.437

Synonyms:2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone

Chemical Property of 2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone

Chemical Property:

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Technology Process of 2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone

There total 2 articles about 2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

N1-ethyl-N1-(2-methoxybenzyl)propane-1,3-diamine (616885-82-6) + 2,5-dimethoxyquinone (3117-03-1) → 2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone (1130608-96-6)

Guidance literature:

at 20 ℃; for 6h;

DOI:10.1021/jm901123n

Reference yield: 40.0%

→ 2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone (1130608-96-6)

Guidance literature:

Reference yield: 91.0%

2-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-5-methoxy-[1,4]benzoquinone (1130608-96-6) + N-Boc-1,3-diaminopropane (75178-96-0) → [3-(4-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-3,6-dioxocyclohexa-1,4-dienylamino)-propyl]-carbamic acid tert-butyl ester (1130608-99-9)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/jm901123n

upstream raw materials:

N₁-ethyl-N₁-(2-methoxybenzyl)propane-1,3-diamine

2,5-dimethoxyquinone

Downstream raw materials:

[6-(4-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-3,6-dioxocyclohexa-1,4-dienylamino)-hexyl]-carbamic acid tert-butyl ester

[3-(4-{3-[ethyl-(2-methoxybenzyl)-amino]-propylamino}-3,6-dioxocyclohexa-1,4-dienylamino)-propyl]-carbamic acid tert-butyl ester

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