C₃₅H₅₉N₃O₈

Base Information

Chemical Name:C₃₅H₅₉N₃O₈
CAS No.:1309922-69-7
Molecular Formula:C₃₅H₅₉N₃O₈
Molecular Weight:649.869
Hs Code.:

C<sub>35</sub>H<sub>59</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₅H₅₉N₃O₈

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Chemical Property of C₃₅H₅₉N₃O₈

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Technology Process of C₃₅H₅₉N₃O₈

There total 14 articles about C₃₅H₅₉N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69-65-8
mannitol

: 1309922-69-7
C₃₅H₅₉N₃O₈

Guidance literature:: Multi-step reaction with 14 steps

1.1: toluene-4-sulfonic acid / acetone / 24 h / Reflux

2.1: hydrogenchloride / water; methanol / 20 °C

3.1: sodium periodate; sodium hydrogencarbonate / water / 3 h / 0 - 8 °C

3.2: 17 h / 20 °C

4.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

5.1: trifluoroacetic acid / acetonitrile; water / 6 h / Reflux

6.1: lithium hexamethyldisilazane; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran / 3 h / -78 °C

6.2: 3 h / -78 °C

7.1: pyridine; trichlorophosphate / 12.5 h / 10 - 20 °C

7.2: 0 °C / pH 5.5

8.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

9.1: n-butyllithium; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran; TETRAHYDROPYRANE / 1.33 h / -78 °C

9.2: 1.33 h / -78 °C

9.3: -78 °C / pH 7

10.1: triethylamine / dichloromethane / -10 °C

11.1: tetra(n-butyl)ammonium hydrogensulfate; sodium azide / N,N-dimethyl-formamide / 36 h / 90 °C

12.1: triethylamine; hydrogen / palladium 10% on activated carbon / ethanol; water / 16 h / 3102.97 Torr

13.1: potassium hydroxide / water; tetrahydrofuran; methanol / 10 h / 0 °C

13.2: 10 h / 0 - 20 °C

14.1: triethylamine; 2-hydroxypyridin / 48 h / 90 °C

With pyridine; 2-hydroxypyridin; hydrogenchloride; sodium periodate; n-butyllithium; sodium azide; N²,N²-dimethyl-2-methyl-1,2-propanediamine; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; potassium hydroxide; lithium hexamethyldisilazane; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; TETRAHYDROPYRANE; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 3969-59-3
mannitol triacetonide

: 1309922-69-7
C₃₅H₅₉N₃O₈

Guidance literature:: Multi-step reaction with 13 steps

1.1: hydrogenchloride / water; methanol / 20 °C

2.1: sodium periodate; sodium hydrogencarbonate / water / 3 h / 0 - 8 °C

2.2: 17 h / 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

4.1: trifluoroacetic acid / acetonitrile; water / 6 h / Reflux

5.1: lithium hexamethyldisilazane; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran / 3 h / -78 °C

5.2: 3 h / -78 °C

6.1: pyridine; trichlorophosphate / 12.5 h / 10 - 20 °C

6.2: 0 °C / pH 5.5

7.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

8.1: n-butyllithium; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran; TETRAHYDROPYRANE / 1.33 h / -78 °C

8.2: 1.33 h / -78 °C

8.3: -78 °C / pH 7

9.1: triethylamine / dichloromethane / -10 °C

10.1: tetra(n-butyl)ammonium hydrogensulfate; sodium azide / N,N-dimethyl-formamide / 36 h / 90 °C

11.1: triethylamine; hydrogen / palladium 10% on activated carbon / ethanol; water / 16 h / 3102.97 Torr

12.1: potassium hydroxide / water; tetrahydrofuran; methanol / 10 h / 0 °C

12.2: 10 h / 0 - 20 °C

13.1: triethylamine; 2-hydroxypyridin / 48 h / 90 °C

With pyridine; 2-hydroxypyridin; hydrogenchloride; sodium periodate; n-butyllithium; sodium azide; N²,N²-dimethyl-2-methyl-1,2-propanediamine; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; triethylamine; trifluoroacetic acid; potassium hydroxide; lithium hexamethyldisilazane; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; TETRAHYDROPYRANE; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 3969-84-4
3,4-di-O-isopropylidene-D-mannitol

: 1309922-69-7
C₃₅H₅₉N₃O₈

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium periodate; sodium hydrogencarbonate / water / 3 h / 0 - 8 °C

1.2: 17 h / 20 °C

2.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

3.1: trifluoroacetic acid / acetonitrile; water / 6 h / Reflux

4.1: lithium hexamethyldisilazane; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran / 3 h / -78 °C

4.2: 3 h / -78 °C

5.1: pyridine; trichlorophosphate / 12.5 h / 10 - 20 °C

5.2: 0 °C / pH 5.5

6.1: hydrogen / palladium 10% on activated carbon / methanol / 3102.97 Torr

7.1: n-butyllithium; N²,N²-dimethyl-2-methyl-1,2-propanediamine / tetrahydrofuran; TETRAHYDROPYRANE / 1.33 h / -78 °C

7.2: 1.33 h / -78 °C

7.3: -78 °C / pH 7

8.1: triethylamine / dichloromethane / -10 °C

9.1: tetra(n-butyl)ammonium hydrogensulfate; sodium azide / N,N-dimethyl-formamide / 36 h / 90 °C

10.1: triethylamine; hydrogen / palladium 10% on activated carbon / ethanol; water / 16 h / 3102.97 Torr

11.1: potassium hydroxide / water; tetrahydrofuran; methanol / 10 h / 0 °C

11.2: 10 h / 0 - 20 °C

12.1: triethylamine; 2-hydroxypyridin / 48 h / 90 °C

With pyridine; 2-hydroxypyridin; sodium periodate; n-butyllithium; sodium azide; N²,N²-dimethyl-2-methyl-1,2-propanediamine; hydrogen; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; triethylamine; trifluoroacetic acid; potassium hydroxide; lithium hexamethyldisilazane; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; TETRAHYDROPYRANE; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;