1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole

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Chemical Name:1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole
CAS No.:1433554-91-6
Molecular Formula:C₁₉H₂₅N₃O₂Si
Molecular Weight:355.512
Hs Code.:

Synonyms:1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole

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Chemical Property of 1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole

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Technology Process of 1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole

There total 2 articles about 1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 71789-10-1
1-trimethylsilyl-1,4-pentadiyne

: 1218787-39-3
benzyl α-azidoisobutyrate

: 1433554-91-6
1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1002/ejoc.201201674

Reference yield:

: 55456-40-1
benzyl 2-aminoisobutyrate

: 1433554-91-6
1-[2-(benzyloxycarbonyl)-2-propyl]-4-[3-(trimethylsilyl)prop-2-ynyl]-1H-1,3,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: triflic azide; triethylamine; copper(ll) sulfate pentahydrate / acetonitrile / 0 - 20 °C / Inert atmosphere

2: copper(l) iodide; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / acetonitrile / 16 h / 20 °C / Inert atmosphere

With copper(l) iodide; copper(ll) sulfate pentahydrate; triflic azide; triethylamine; N-ethyl-N,N-diisopropylamine; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In acetonitrile;
DOI:10.1002/ejoc.201201674