7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

Base Information

Chemical Name:7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene
CAS No.:914336-59-7
Molecular Formula:C₂₄H₂₀N₄O₂
Molecular Weight:396.448
Hs Code.:

Synonyms:7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

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Chemical Property of 7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

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Technology Process of 7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

There total 7 articles about 7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 914262-92-3
7-(4'-cyanobiphenyl-4-yl)-2-cyanonaphthalene

: 914336-59-7
7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

Guidance literature:: With hydroxylamine hydrochloride; potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.bmc.2006.07.024

Reference yield:

: 914262-90-1
7-(4-bromophenyl)-2-cyanonaphthalene

: 914336-59-7
7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / tetrabutylammonium fluoride; potassium carbonate / palladium(II) acetate / H₂O; 1,2-dimethoxy-ethane / 3 h / Heating

2: 96 percent / hydroxylamine hydrochloride; potassium tert-butoxide / dimethylsulfoxide / 20 °C

With hydroxylamine hydrochloride; potassium tert-butylate; tetrabutyl ammonium fluoride; potassium carbonate; palladium diacetate; In 1,2-dimethoxyethane; water; dimethyl sulfoxide; 1: Suzuki coupling;
DOI:10.1016/j.bmc.2006.07.024

Reference yield:

: 5060-82-2
7-methoxy-2-naphthol

: 914336-59-7
7-(4'-N-hydroxyamidinobiphenyl-4-yl)-2-N-hydroxyamidinonaphthalene

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / pyridine / toluene / 2 h / 20 °C

2: 82 percent / tetrakis(triphenylphosphine)palladium / dimethylformamide / 3 h / 150 °C

3: 80 percent / BBr₃ / CH₂Cl₂ / 48 h / 20 °C

4: 79 percent / pyridine / toluene / 2 h / 20 °C

5: 88 percent / tetrabutylammonium fluoride; potassium carbonate / palladium(II) acetate / H₂O; 1,2-dimethoxy-ethane / 1 h / 20 °C

6: 88 percent / tetrabutylammonium fluoride; potassium carbonate / palladium(II) acetate / H₂O; 1,2-dimethoxy-ethane / 3 h / Heating

7: 96 percent / hydroxylamine hydrochloride; potassium tert-butoxide / dimethylsulfoxide / 20 °C

With pyridine; hydroxylamine hydrochloride; potassium tert-butylate; tetrabutyl ammonium fluoride; boron tribromide; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; In 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 5: Suzuki coupling / 6: Suzuki coupling;
DOI:10.1016/j.bmc.2006.07.024