1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

Base Information

Chemical Name:1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide
CAS No.:132532-32-2
Molecular Formula:C₁₇H₂₃N₃O₂
Molecular Weight:301.389
Hs Code.:

Synonyms:1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

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Chemical Property of 1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

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Technology Process of 1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

There total 1 articles about 1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 42833-31-8
4-(1-methyl-1,2,3,6-tetrahydropyridin-4-yl)morpholine

: 103-71-9
phenyl isocyanate

: 132532-32-2
1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

Guidance literature:: In acetone; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81468-X

Reference yield: 74.0%

: 132532-32-2
1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

: 132532-33-3
5-chloro-1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

Guidance literature:: With N-chloro-succinimide; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.1016/S0040-4020(01)81468-X

Reference yield:

: 132532-32-2
1,2,3,6-tetrahydro-1-methyl-4-morpholino-N-phenyl-3-pyridinecarboxamide

: 132532-34-4
5-morpholino-4-phenylimino-3,8-diazatricyclo<4.3.0.0^1.5>nonan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / N-chlorosuccinimide / CH₂Cl₂ / 2.5 h / 20 °C

2: 51 percent / methanol; H₂O / 17 h / 60 °C

With N-chloro-succinimide; In methanol; dichloromethane; water;
DOI:10.1016/S0040-4020(01)81468-X