N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide

Base Information

Chemical Name:N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide
CAS No.:4826-44-2
Molecular Formula:C₁₇H₂₀N₂O₂
Molecular Weight:284.358
Hs Code.:

Synonyms:N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide

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Chemical Property of N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide

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Technology Process of N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide

There total 2 articles about N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 67462-20-8
(1R,2S)-N-amino-2-methylamino-1-phenyl-1-propanol

: 93-97-0
benzoic acid anhydride

: 4826-44-2
N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide

Guidance literature:: (1R,2S)-N-amino-2-methylamino-1-phenyl-1-propanol; With triethylamine; In dichloromethane; at 0 ℃; for 0.0833333h; Inert atmosphere;

benzoic acid anhydride; In dichloromethane; Inert atmosphere;
DOI:10.1002/jhet.402

Reference yield:

: 1850-68-6,4826-44-2
N-Benzoylamino-l-ephedrin

Guidance literature:: N-Amino-l-ephedrin, Benzoylchlorid, Py., Toluol (6h, ca. 100grad);
DOI:10.1021/jo01026a035

Reference yield: 36.0%

: 4826-44-2
N'-((1S,2R)-2-hydroxy-1-methyl-2-phenylethyl)-N'-methyl benzoic acid hydrazide

: 4826-46-4
trans-(5S,6S)-4,5-dimethyl-2,6-diphenyl-5,6-dihydro-4H-1,3,4-oxadiazine

: 4826-49-7
cis-(5S,6R)-4,5-dimethyl-2,6-diphenyl-5,6-dihydro-4H-1,3,4-oxadiazine

Guidance literature:: With hydrogen bromide; In propionic acid; for 24h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/jhet.402