2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

Base Information

• Chemical Name: 2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane
• CAS No.: 1305033-17-3
• Molecular Formula: C₁₇H₂₅BO₄
• Molecular Weight: 304.194
• Mol file: 1305033-17-3.mol

Synonyms:2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

Chemical Property of 2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

Chemical Property:

Purity/Quality:

99%,98%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

There total 1 articles about 2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

4-formylphenylboronic acid, (87199-17-5) + 2,2-Dimethyl-1,3-propanediol (126-30-7) → 2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane (1305033-17-3)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; at 115 ℃; Inert atmosphere;

DOI:10.1039/d0cc08129a

Reference yield: 53.0%

2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane (1305033-17-3) + 4,4'-(3,6-dibromo-9H-fluorene-9,9-diyl)dianiline → 4,4'-(3,6-bis(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-9H-fluorene-9,9-diyl)dianiline

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; water; at 100 ℃; for 24h; Inert atmosphere;

DOI:10.1039/d0cc08129a

Reference yield: 52.0%

2-(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane (1305033-17-3) + 3,3’-dibromo-9,9’-bicarbazole → 3,3'-bis(4-(5,5-dimethyl-1,3-dioxan-2-yl)phenyl)-9,9'-bicarbazole

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; water; toluene; at -196.16 - 100 ℃; for 24h;

DOI:10.1002/chem.202001385

upstream raw materials:

4-formylphenylboronic acid,

2,2-Dimethyl-1,3-propanediol

Downstream raw materials:

C₃₁H₂₈N₂O₃

C₂₄H₂₁BrN₂O₂