(NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

Base Information

Chemical Name:(NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}
CAS No.:95674-06-9
Molecular Formula:C₁₆H₃₆N*C₄₀H₁₀AgF₃₀OPt₂
Molecular Weight:1816.97
Hs Code.:

Synonyms:(NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

Chemical Property:

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Technology Process of (NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

There total 3 articles about (NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 116349-58-7
(NBu4)2{platinum2(μ-pentafluorophenyl)2(pentafluorophenyl)4}

: silver perchlorate

: 95674-06-9
(NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

: 1923-70-2
tetrabutylammonium perchlorate

Guidance literature:: In diethyl ether; dichloromethane; Addn. of AgClO4 to a CH2Cl2 soln. of Pt-complex (molar ratio 1:1) and stirring of mixt. (exclusion of light, room temp., 1 h).; Evapn. of soln. to dryness and treatment of resulting oily residue with O(C2H5)2 to separate the insoluble org. compd. Evapn. of ether soln. to dryness gives a solid.;

Reference yield: 72.0%

: 90621-02-6
(NBu₄)2{platinum(pentafluorophenyl)3Cl}

: silver perchlorate

: 95674-06-9
(NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

: 1923-70-2
tetrabutylammonium perchlorate

: silver(I) chloride

Guidance literature:: In diethyl ether; dichloromethane; Addn. of AgClO4 to a CH2Cl2 soln. of Pt-complex (molar ratio 2:1) and stirring of mixt. (exclusion of light, room temp., 2 h).; Filtn. of formed AgCl and of excess of AgClO4, evapn. of resulting yellow soln. to dryness and washing of obtained oily residue with O(C2H5)2 to separate the insoluble org. compd. Partial evapn. of yellow soln. and addn. of n-hexane gives a solid.;

Reference yield:

: (C₄H₉)4N⁽¹⁺⁾*Pt₂Ag(C₆F₅)6(C₂H₅)2O^(1-)*(C₂H₅)2O=[N(C₄H₉)4][Pt₂Ag(C₆F₅)6(C₂H₅)2O]*(C₂H₅)2O

: 95674-06-9
(NBu4){platinum2(silver)(μ-pentafluorophenyl)2(pentafluorophenyl)4(diethyl ether)}

Guidance literature:: In neat (no solvent, solid phase); byproducts: (C2H5)2O; starting compd. loses 1 molecule of Et2O after 30 min at 80°C;;
DOI:10.1021/ja00294a062