(E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

Base Information

Chemical Name:(E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide
CAS No.:954426-16-5
Molecular Formula:C₂₁H₂₂N₄O₄S
Molecular Weight:426.496
Hs Code.:

Synonyms:(E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

Suppliers and Price of (E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

Chemical Property:

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Technology Process of (E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

There total 3 articles about (E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1485-71-8
benzophenone oxime

: (2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)propenoyl chloride hydrochloride

: 954426-16-5
(E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

Guidance literature:: With sodium sulfate; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/ol0711568

Reference yield:

: 574-66-3
Benzophenone oxime

: 954426-16-5
(E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / aq. HCl; NaBH₃CN / methanol / 4 h / 20 °C / pH 3

2: 6.94 g / Na₂SO₄; Et₃N / CH₂Cl₂ / 20 °C

With hydrogenchloride; sodium cyanoborohydride; sodium sulfate; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ol0711568

Reference yield:

: 610768-51-9
(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)propenoic acid

: 954426-16-5
(E)-N-benzhydryl-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-N-hydroxy-2-propenamide

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride; DMF / CH₂Cl₂ / 2 h / 20 °C

2: 6.94 g / Na₂SO₄; Et₃N / CH₂Cl₂ / 20 °C

With oxalyl dichloride; sodium sulfate; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1021/ol0711568