5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole
CAS No.:854000-00-3
Molecular Formula:C₁₉H₃₂N₄O₃SSi
Molecular Weight:424.64
Hs Code.:

Synonyms:5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

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Chemical Property of 5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

Chemical Property:

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Technology Process of 5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

There total 6 articles about 5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 75-77-4
chloro-trimethyl-silane

: 853999-99-2
3-methyl-1-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]octan-3-ol

: 854000-00-3
5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/j.bmc.2017.11.035

Reference yield:

: C₁₆H₂₆O₄S

: 854000-00-3
5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3.5 h / 60 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

3: 1H-imidazole / dichloromethane / 1 h / 0 °C

With 1H-imidazole; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2017.11.035

Reference yield:

: 110-43-0
n-pentyl methyl ketone

: 854000-00-3
5-({3-methyl-3-[(trimethylsilyl)oxy]octyl}sulfonyl)-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 6 steps

1: zinc; iodine / 1,4-dioxane / 2 h / 0 - 20 °C / Sonication

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.58 h / 0 °C

3: sodium hydroxide; tetrabutylammomium bromide / toluene / 1 h / 0 - 20 °C

4: toluene / 3.5 h / 60 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

6: 1H-imidazole / dichloromethane / 1 h / 0 °C

With 1H-imidazole; lithium aluminium tetrahydride; tetrabutylammomium bromide; iodine; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene; 1: |Reformatsky Reaction;
DOI:10.1016/j.bmc.2017.11.035