4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

Base Information

Chemical Name:4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride
CAS No.:75244-02-9
Molecular Formula:C₂₂H₂₇N₃O₅*ClH
Molecular Weight:449.934
Hs Code.:

Synonyms:4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

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Chemical Property of 4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

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Technology Process of 4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

There total 4 articles about 4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 33477-30-4
4-nitrobenzyl ester of N-t-butyloxycarbonyl-L-phenylalanyl-L-leucine

: 75244-02-9
4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 0.75h;

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 75244-02-9
4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / N,N'-dicyclohexylcarbodiimide (DCCI) / tetrahydrofuran / Ambient temperature

2: 1.) NH₃, 2.) AcOH / 1.) CHCl₃, 5 min, 2.) THF, 20 h

3: 98 percent / 4M HCl / dioxane / 0.75 h

With hydrogenchloride; ammonia; acetic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 81638-94-0
O-(t-butyloxycarbonyl-L-phenylalanyl)-2-pyridylmethylketoxime

: 75244-02-9
4-nitrobenzyl ester of L-phenylalanyl-L-leucine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NH₃, 2.) AcOH / 1.) CHCl₃, 5 min, 2.) THF, 20 h

2: 98 percent / 4M HCl / dioxane / 0.75 h

With hydrogenchloride; ammonia; acetic acid; In 1,4-dioxane;