methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

Base Information

Chemical Name:methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester
CAS No.:1150560-58-9
Molecular Formula:C₁₅H₂₃NO₅S
Molecular Weight:329.417
Hs Code.:

Synonyms:methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

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Chemical Property of methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

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Technology Process of methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

There total 9 articles about methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 124-63-0
methanesulfonyl chloride

: 718611-17-7
S-(3-hydroxy-1-phenyl-propyl)-carbamic acid tert-butyl ester

: 1150560-58-9
methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 10 ℃; for 1h; Large scale;

Reference yield:

: 82769-76-4
(S)-3-amino-3-phenylpropanol

: 1150560-58-9
methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 8 h / 20 °C

2: pyridine / 0 - 20 °C

With pyridine; In dichloromethane;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1150560-58-9
methanesulfonic acid (S)-3-tert-butoxycarbonylamino-3-phenylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: pyridine / 0 - 20 °C

With pyridine; triethylamine; In dichloromethane;