(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Base Information

Chemical Name:(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione
CAS No.:168132-73-8
Molecular Formula:C₃₅H₄₀N₂O₈
Molecular Weight:616.711
Hs Code.:

Synonyms:(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

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Chemical Property of (Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

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Technology Process of (Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

There total 1 articles about (Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.8%

: 108-23-6
isopropyl chloroformate

: 168132-72-7
1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

: 168132-73-8
(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/0040-4020(95)00437-D

Reference yield:

: 168132-73-8
(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: 168132-72-7
1-Benzyl-3-(4-methoxy-3-methyl-benzyl)-6-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-2,5-dione

: 4-Benzyl-2-hydroxy-6-(4-methoxy-3-methyl-benzyl)-5-oxo-3-[1-(2,4,5-trimethoxy-3-methyl-phenyl)-meth-(Z)-ylidene]-piperazine-1-carboxylic acid isopropyl ester

Guidance literature:: With lithium tri(t-butoxy)aluminum hydride; In tetrahydrofuran; at 0 ℃; for 1h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0040-4020(95)00437-D

Reference yield:

: 168132-73-8
(Z)-1-<(isopropyloxy)carbonyl>-4-benzyl-6-(4-methoxy-3-methylphenylmethyl)-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione

: (E)-3-benzyl-2-<(1,2,3,4,5,6-hexahydro-2,4,5-trimethoxy-3-methylphenyl)methylene>-9-methoxy-8-methyl-1,5-imino-3-benzazocine

: C₃₁H₃₄N₂O₅

Guidance literature:: With lithium tri(t-butoxy)aluminum hydride; sulfuric acid; trifluoroacetic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, 0 deg C, 1 h, 2.) RT, 70 h;
DOI:10.1016/0040-4020(95)00437-D