3--1-naphtol

Base Information

• Chemical Name: 3--1-naphtol
• CAS No.: 99647-86-6
• Molecular Formula: C₁₇H₁₄O
• Molecular Weight: 234.298
• Mol file: 99647-86-6.mol

Synonyms:3--1-naphtol

Chemical Property of 3--1-naphtol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3--1-naphtol

There total 13 articles about 3--1-naphtol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-(2-methylphenyl)-3-(4-methylphenyl)prop-2-yn-1-one → 3--1-naphtol (99647-86-6)

Guidance literature:

With copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; at 20 ℃; for 24h; Irradiation; Inert atmosphere; Schlenk technique;

DOI:10.1021/acs.orglett.0c01854

Reference yield: 94.0%

C26H22OP(1+)*CF3O3S(1-) + 1-(((dimethyl(oxo)- λ6-sulfanylidene)methyl)sulfonyl)-4-methylbenzene → 3--1-naphtol (99647-86-6)

Guidance literature:

With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; sodium acetate; In ethanol; at 120 ℃; for 10h; Inert atmosphere;

DOI:10.1039/d1cc00433f

Reference yield: 92.0%

1-(2-[(4-methylphenyl)ethynyl]phenyl)ethanone (1262832-17-6) → 3--1-naphtol (99647-86-6)

Guidance literature:

With cesium acetate; copper(l) chloride; In 1,4-dioxane; at 120 ℃; for 12h; regioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1002/chem.201901860

upstream raw materials:

4-chloronaphthalen-1-ol

toluene

α-naphthol

1-(4-methylphenyl)butan-1,3-dione