FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5

Base Information

Chemical Name:FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5
CAS No.:81987-86-2
Molecular Formula:C₅₃H₄₀FeIrO₅P₃
Molecular Weight:1097.89
Hs Code.:

FeIrP(C<sub>6</sub>H<sub>5</sub>)2(P(C<sub>6</sub>H<sub>5</sub>)3)2(CO)5

Synonyms:FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5

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Chemical Property of FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5

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Technology Process of FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5

There total 7 articles about FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 18399-66-1,38967-68-9
Fe(CO)4(PH(C₆H₅)2)

: 81987-86-2
FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5

Guidance literature:: With n-butyllithium; In tetrahydrofuran; byproducts: LiCl; n-BuLi was added to a THF soln. of Fe-complex, the soln. was slowly added to a THF soln. of Ir-complex, the soln. was stired for 3 h at 25°C;; extd. with toluene, chromd. on alumina with CH2Cl2-hexane under N2;;

Reference yield: 37.0%

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 82042-06-6
Li[PPh₂Fe(CO)4]

: 81987-86-2
FeIrP(C₆H₅)2(P(C₆H₅)3)2(CO)5

: 85185-78-0
FeIr(μ-PPh2)(CO)6(PPh3)

Guidance literature:: In tetrahydrofuran; THF soln. of Fe complex was slowly added under N2 to suspn. of Ir complex in THF; stirring at 23°C for 3 h; evapn., extn. with toluene, exts. were filtered and concd.; chromy. on alumina (CH2Cl2/hexane) under N2; elem. anal.;