meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Base Information

Chemical Name:meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine
CAS No.:730992-56-0
Molecular Formula:C₂₈H₁₈F₁₀N₂O₂
Molecular Weight:604.447
Hs Code.:

Synonyms:meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

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Technology Process of meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

There total 3 articles about meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 153255-91-5
(E)-N-(4-methoxyphenyl)-1-(perfluorophenyl) methanimine

: 730992-56-0
meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

: (+/-)-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Guidance literature:: With copper; (+)-10-camphorsulfonic acid; zinc; In tetrahydrofuran; at 20 ℃; for 6h;
DOI:10.1246/bcsj.77.1001

Reference yield:

: 653-37-2
perfluorobenzaldehyde

: 730992-56-0
meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / CH₂Cl₂ / 3 h / 20 °C

2: 31 percent / Zn-Cu; (+)-camphorsulfonic acid / tetrahydrofuran / 6 h / 20 °C

With copper; (+)-10-camphorsulfonic acid; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.77.1001

Reference yield:

: 104-94-9
4-methoxy-aniline

: 730992-56-0
meso-N,N'-bis(4-methoxyphenyl)-1,2-bis(pentafluorophenyl)ethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / CH₂Cl₂ / 3 h / 20 °C

2: 31 percent / Zn-Cu; (+)-camphorsulfonic acid / tetrahydrofuran / 6 h / 20 °C

With copper; (+)-10-camphorsulfonic acid; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1246/bcsj.77.1001