3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid

Base Information

Chemical Name:3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid
CAS No.:265130-75-4
Molecular Formula:C₂₇H₂₆O₆
Molecular Weight:446.5
Hs Code.:

Synonyms:3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid

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Chemical Property of 3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid

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Technology Process of 3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid

There total 2 articles about 3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.2%

: 265130-74-3
ethyl 3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2-ethoxypropionate

: 265130-75-4
3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid

Guidance literature:: With sodium hydroxide; In ethanol; at 90 ℃; for 1h;
DOI:10.1021/jm010964g

Reference yield:

: 197299-16-4
ethyl 2-ethoxy-3-(4-hydroxy-phenyl)-propionate

: 265130-75-4
3-(4-(2-(12H-dibenzo[d,g]-1,3-dioxocine-12-ylidene)ethoxy)phenyl)-2ethoxypropionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 8.5 h / 60 °C / Heating / reflux

2: sodium hydroxide / ethanol; water / 2 h / 20 °C

With sodium hydroxide; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;