1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane

Base Information

• Chemical Name: 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane
• CAS No.: 138426-39-8
• Molecular Formula: C₁₇H₁₄F₁₃ISi
• Molecular Weight: 620.267

Synonyms:1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane

Chemical Property of 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane

Chemical Property:

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Technology Process of 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane

There total 3 articles about 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

n-perfluorohexyl iodide (355-43-1) + 1-phenyl-1-vinyl-1-silacyclobutane (74045-43-5) → 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane (138426-39-8)

Guidance literature:

With triethyl borane; In hexane;

DOI:10.1016/0040-4039(91)80175-6

Reference yield:

1-chloro-1-phenyl-1-silacyclobutane (3401-28-3) → 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane (138426-39-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / 3 h / 0 °C

2: 90 percent / triethylborane / hexane / 10 h / 25 °C

With triethyl borane; In tetrahydrofuran; hexane;

DOI:10.1246/bcsj.68.250

Reference yield:

dichloro(3-chloropropyl)phenylsilane (3401-26-1) → 1-phenyl-1-(3,3,4,4,5,5,6,6,7,7,8,8,8-trodecafluoro010iodooctyl)silacyclobutane (138426-39-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Mg, 1,2-dibromoethane / 1.) THF, reflux, 2 h, 2.) THF, 0 deg C, 1 h

2: 90 percent / triethylborane / hexane / 10 h / 25 °C

With triethyl borane; magnesium; ethylene dibromide; In hexane;

DOI:10.1246/bcsj.68.250

upstream raw materials:

n-perfluorohexyl iodide

1-phenyl-1-vinyl-1-silacyclobutane

dichloro(3-chloropropyl)phenylsilane

1-chloro-1-phenyl-1-silacyclobutane

Downstream raw materials:

1-t-butoxy-1-phenyl-2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl)silacyclopentane

1-acetoxy-1-phenyl-2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoroheptyl)silacyclopentane

(1R,2S)-1-tert-Butoxy-1-phenyl-2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoro-heptyl)-silolane

(1S,2S)-1-tert-Butoxy-1-phenyl-2-(2,2,3,3,4,4,5,5,6,6,7,7,7-tridecafluoro-heptyl)-silolane

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